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Autotap™ and Dual Autotap™:
Tap Density Analyzers

Options | Tap Density | Hausner/Carr’s | Geometric Density | Feature Article
Specifications | Lab Services | References | Standard Methods


Tap density of powders, granules, flakes and other finely divided solids is an important characteristic and commonly measured property of numerous materials.  The Autotap automates the lifting and dropping of the powder container (usually a glass graduated measuring cylinder) thereby eliminating both the expected variability and possible wrist injury when done by hand, not least because most materials require hundreds if not thousands of taps before reaching maximum tapped density.

Available Options
The Autotaps are normally supplied with 250ml cylinders, but you may request 10ml, 25ml, 50ml, 100ml or 50ml instead.  A larger optional platform is required to accommodate the largest cylinder we offer, the 1000ml.  But, of course, this platform does accommodate all the smaller cylinders too.  If you need to ensure the same fixed number of taps for all analyses, an optional special lockout feature is also available which prevents unauthorized changes to the counter.

Tap (Tapped) Density

Both Autotaps conform to a number of international standards for tap density, namely ASTM B527, D4164 and D4781, plus British Pharmacopoeia method for Apparent Volume, USP <616> method II, and ISO 787-11. The unique platforms accommodate different size cylinders for different standards and for differing amounts of available sample.

Most samples are analyzed "as-is", normally there is no special preparation needed, just pour the powder into a suitably sized cylinder. Securing (and releasing) the cylinder(s) on the platform(s) is both easy and rapid. Then just dial in the desired number of taps and press "start". Tapping ceases automatically after the prescribed number of taps.

Hausner Ratio & Carr's
Compressibility Index

By comparing the initial (loose) powder volume with the final (tapped) volume one can predict the flowability of a powder.  This comparison is normally done by calculating the ratio of the volumes (Hausner) or the change in volume as a percentage of the initial volume (Carr’s).  For more details, please request our technote  No.30 " Tapped Density in the Pharmaceutical Industry" here

Geometric (envelope) density
Sometimes called particle density or apparent density, the geometric density reflects the volume of particles including internal pores and small surface irregularities.  Important, therefore, for a host of manufactured and natural porous materials it is simply and inexpensively measured using a dry powder pycnometer attachment for the Autotap and either a coarse or fine pycnometric powder, according to the scale of pore size and surface features under test.  For more details, please request our technote No.24 " Geometric (Envelope) Density without Mercury (Tap Density)" here

Feature Article: "The Role of Porosity"
...bulk volume can be determined by Dry Powder Pycnometry. This technique entails measuring the increase in volume of a packed bed of powder when the sample is immersed in it, Archimedes style". more...

Specifications

  • Available as 110-220V/60Hz or 220-240V/50Hz
  • Tap height: 0.125 inch or 3mm
  • Tapping rate: 260 per minute
  • Tap counter: 1- 9999 with auto-stop
  • Continuous tapping: yes, if so desired (manual stop)
  • Platform rotation: automatic
  • Controls: on/off, start, stop, counter reset.
  • Load limit: 900g (2lb) with no effect on tapping rate.

    • -1800g (4lb) with 5% reduction in tapping rate

      -2275g (5lb) with 15%reduction in tapping rate
Laboratory Services

Tap density, Hausner Ratio, Carr's Index and Geometric Density are just a few of the measurements offered by our Applications Laboratory on a fee basis. Click here
for more details including sample submission instructions.

Those seriously considering the purchase of an instrument may request free evaluation analyses (no more than two please) or a demonstration in their facility.  Please make your requests using this form

A Note on Standard Methods
Because of copyright restrictions, Quantachrome cannot provide copies of standards published by other organizations such as ASTM International.  However they are available for purchase online, together with those of ISO and DIN, at techstreet.com: http://www.techstreet.com/cgi-bin/joint.cgi/426039/cgi-bin/publisher

Autotap and Dual Autotap Analyzers

References*
The following papers cite the use of Quantachrome's Autotap tap density analyzers. These represent just a few of all such papers. If you would like an extended list, please contact us

*Due to copyright restrictions, Quantachrome cannot provide copies of these or other papers, but we will gladly assist you in obtaining copies from the authors if you encounter difficulties.

"Influence of process parameters on the tapping characteristics of high shear mixer agglomerates made with ultra-high viscosity binders"
S.L.Rough, D.I.Wilson, A.E.Bayly and D.W.York (2005) Chemical Engineering Research and Design, 83, 7-23

"Investigation of various factors affecting encapsulation on the in-cap automatic capsule-filling machine"
R. Nair, M.Vemuri, P.Agrawala and S-I.Kim (2004) AAPS PharmSciTech, 5(4) Article 57

"Characterization of flow properties of powder coatings used in the automotive industry"
C.Conesa et al  (2004) KONA, 22, 94-106

"Interparticle van der Waals force in powder flowability and compactibility"
Q.Li, V.Rudolph, B.Weigl and A.Earl (2004) International Journal of Pharmaceutics, 280, 77-93

"Effect of alumina particle size and distribution on infiltration rate and fracture toughness of alumina–glass composites prepared by melt infiltration"
D-Y.Lee, D-J.Kim, B-Y.Kim and Y-S.Song (2003) Materials Science and Engineering A, 341, 98-105

"The effect of formulation variables on the dissolution and physical properties of spray-dried microspheres containing organic salts"
F.Oneda and M.I.Ré (2003) Powder Technology, 130, 377-384

"Effect of mixing on the rheology and particle characteristics of tungsten-based powder injection molding feedstock"
P.Suri, S.V.Atre, R.M.German and J.P.deSouza (2003) Materials Science and Engineering A, 356, 337-344

"Characterization of melt-derived 45S5 and sol-gel-derived 58S bioactive glasses"
P.Sepulveda, J.R.Jones, and L.L.Hench (2001) Journal of Biomedical Materials Research, Applied Biomaterials, 58, 734-740

"Effect of polymer compositions on the fabrication of poly(ortho-ester) microspheres for controlled release of protein"
X-L.Bai et al (2001) Journal of Applied Polymer Science, 80, 1630-1642
 
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