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ASTM STANDARD METHODS

ASTM STANDARD METHODS APPLICABLE TO THE CHARACTERIZATION OF POROUS SOLIDS USING QUANTACHROME INSTRUMENTS.

Gas Physisorption

Surface Area

C1274-12

Standard Test Method for Advanced Ceramic Specific Surface Area by Physical Adsorption.

C1251-95

Standard guide for determination of Specific Surface Area of Advanced Ceramic Materials by Gas Adsorption (withdrawn 2000) .

C1069-09

Standard Test Method for Specific Surface Area of Alumina or Quartz by Nitrogen Adsorption.

D1993-03(2008)

Standard Test Method for Precipitated Silica - Surface Area by Multipoint BET Nitrogen Adsorption.

D5604-96(2012)

Standard Test Methods for Precipitated Silica - Surface Area by Single Point B.E.T. Nitrogen Adsorption.

D6556-10

Standard Test Method for Carbon Black-Total and External Surface Area by Nitrogen Adsorption D4820-99 Standard Test Methods for Carbon Black Surface Area by Multipoint B.E.T. Nitrogen Adsorption (withdrawn 2000)D5816-99 Standard Test Methods for Carbon Black - External Surface Area by Multipoint Nitrogen Adsorption (withdrawn 2000) D3037-93 Standard Test Methods for Carbon Black - Surface Area by Nitrogen Adsorption (withdrawn 1999).

D4567-03(2013)

Standard Test Method for Single-Point Determination of Specific Surface Area of Catalysts and Catalyst Carriers Using Nitrogen Adsorption by Continuous Flow Method.

D4780-12

Standard Test Method for Determination of Low Surface Area of Catalysts and Catalyst Carriers by Multipoint Krypton AdsorptionD3663-03(2008) Standard Test Method for Surface Area of Catalysts and Catalyst Carriers.

B922-10

Standard Test Method for Metal Powder Specific Surface Area by Physical Adsorption.

Pore Volume, Pore Size and Pore Size Distribution

D4365-13

Standard Test Method for Determining Micropore Volume and Zeolite Area of a Catalyst.

D4222-03(2008)

Standard Test Method for Determination of Nitrogen Adsorption and Desorption Isotherms of Catalysts by Static Volumetric Measurements.

D4641-12

andard Practice for Calculation of Pore Size Distributions of Catalysts and Catalyst Carriers from Nitrogen Desorption Isotherms.

CHEMISORPTION

D4824-13

Standard Test Method for Determination of Catalyst Acidity by Ammonia Chemisorption.

D3908-03(2008)

Standard Test Method for Hydrogen Chemisorption on Supported Platinum Catalysts by Volumetric Vacuum MethodD5160-95(2008) Standard Guide for Gas-Phase Adsorption Testing of Activated Carbon

D5228-92(2010)

Standard Test Method for Determination of Butane Working Capacity of Activated Carbon

D5742-95(2010)

Standard Test Method for Determination of Butane Activity of Activated Carbon.

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DRAFTS

WK17122

Test Method for Carbon Monoxide on Supported Platinum on Alumina Catalysts using Manometric Method.

WK17123

Test Method for Carbon Monoxide Chemisorption on Supported Platinum on Alumina Catalysts using Dynamic Flow Method.

MERCURY POROSIMETRY: PORE VOLUME / PORE SIZE / PORE SIZE DISTRIBUTION

D4404-10 

Standard Test Method for Determination of Pore Volume and Pore Volume Distribution of Soil and Rock by Mercury Intrusion Porosimetry.

D4284-12

Standard Test Method for Determining Pore Volume Distribution of Catalysts and Catalyst Carriers by Mercury Intrusion Porosimetry.

D2873-94(1999) e1

Standard Test Method for Interior Porosity of Poly(Vinyl Chloride) (PVC) Resins by Mercury Intrusion Porosimetry (withdrawn 2003).

C493-98

Standard Test Method for Bulk Density and Porosity of Granular Refractory Materials by Mercury Displacement (withdrawn 2002).

D6761-07(2012)

Standard Test Method for Determination of the Total Pore Volume of Catalysts and Catalyst Carriers.

HELIUM PYCNOMETRY: TRUE DENSITY, OPEN- AND CLOSED CELL CONTENT

D2638-10

Standard Test Method for Real Density of Calcined Petroleum Coke by Helium Pycnometer.

D5550-10

Standard Test Method for Specific Gravity of Soil Solids by Gas Pycnometer.

D4892-89(2009)

Standard Test Method for Density of Solid Pitch (Helium Pycnometer Method).

D6093-97(2011)

Standard Test Method for Percent Volume Nonvolatile Matter in Clear or Pigmented Coatings using a Helium Gas Pycnometer.

D5965-02(2013)

Standard Test Methods for Specific Gravity of Coating Powders ; [Note: this test method covers three procedures for determining the specific gravity, method B uses He-Pycnometry].

D6226-10

Standard Test Method for Open Cell Content of Rigid Cellular Plastics.

B923-10

Standard Test Method for Metal Powder Skeletal Density by Helium or Nitrogen Pycnometry.

OTHER STANDARDS RELEVANT TO THE HELIUM PYCNOMETRY

MPIF Standard Test Methods 63-2012 Edition -
Density Determination of Metal Injection Molded (MIM) Components (Gas Pycnometer) .

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TAPPED PACKING DENSITY/BULK DENSITY

D4781-03(2013)

Standard Test Method for Mechanically Tapped Packing Density of Fine Catalyst Particles and Catalyst Carrier Particles.

D4164-13

Standard Test Method for Mechanically Tapped Packing Density of Formed Catalyst and Catalyst Carriers.

B527-06

Standard Test Method for Determination of Tap Density of Metallic Powders and Compounds.

C493-98

Standard Test Method for Bulk Density and Porosity of Granular Refractory Materials by Mercury Displacement (withdrawn 2002).

OTHER STANDARDS RELEVANT TO THE TAPPED DENSITY OF POROUS SOLIDS

JIS K 5101-12-2:2004  Test methods for pigments -- Part 12: Apparent density or apparent specific volume -- Section 2: Mechanically tamped packing method.

JIS-Z-2512 - 2012 EDITION Metallic Powders - Determination of Tap Density.

MPIF Standard Test Methods 46-2012 Edition - Determination of Tap Density of Metal Powders

USP<616> BULK DENSITY AND TAPPED DENSITY OF POWDERS.

MHLW JP 3.01 Determination of Bulk and Tapped Densities Part 2: Method 1[Note: Pharmaceutical powders].

EUROPEAN PHARMACOPOEIA 6.8 Method 1 [Note: Pharmaceutical powders].

SAMPLING

C1069-09

Standard Test Method for Specific Surface Area of Alumina or Quartz by Nitrogen Adsorption
[Note: here the spinning riffler is mentioned].

MPIF 01

Sampling Metal Powderd.

ISO STANDARDS APPLICABLE TO THE CHARACTERIZATION OF POROUS SOLIDS USING QUANTACHROME INSTRUMENTS

ISO 787-11:1981

General methods of tests of pigments and extenders-Part11: Determination of tapped volume and apparent density after tapping.

ISO 9277:2010  

Determination of the specific surface area of solids by gas adsorption -BET method.

ISO 4590:2002

Rigid cellular plastics- Determination of the volume percentage of open cells and closed cells.

ISO 3953:2011

Metallic powders-Determination of tap density.

ISO 18757:2003

Fine ceramics (advanced ceramics, advanced technical ceramics) – Determination of specific surface area of ceramic powders by gas adsorption using the BET method.

ISO 4652:2012

Rubber compounding ingredients -- Carbon black -- Determination of specific surface area by nitrogen adsorption methods -- Single-point procedures.

ISO 5794-1:2010

Rubber compounding ingredients – Silica, precipitated, hydrated - Part 1: Non-Rubber Tets.

ISO 15901-1:2005

Pore size distribution and porosity of solid materials by mercury porosimetry and gas adsorption – Part 1: Mercury Porosimetry.

Note: this standard is currently under revision and is an updated document is available as Draft International Standard (DIS).

ISO 15901-2:2006

Pore size distribution and porosity of solid materials by mercury porosimetry and gas sorption –
Part 2: Analysis of mespores by gas adsorption.

ISO 15901-3:2007

Pore size distribution and porosity of solid materials by mercury porosimetry and gas sorption – Part 3: Analysis of micropores by gas adsorption .

ISO 8460:1987

Instant coffee - Determination of free-flow and compacted bulk densities.

ISO 8967:2005
(IDF 134: 2005)

Dried milk and dried milk products - Determination of bulk density.

ISO 9161:2004

Uranium dioxide powder - Determination of apparent density and tap density.

ISO/FDIS 12154

Determination of density by volumetric displacement -- Skeleton density by gas pycnometry
[Note: this standard will be published in the first half of 2014.. it’s current status is Final Draft International Standard].

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DIN STANDARDS APPLICABLE TO THE CHARACTERIZATION OF POROUS SOLIDS USING QUANTACHROME INSTRUMENTS

DIN 66133
(1993-06)

Determination of pore volume distribution and specific surface area of solids by mercury intrusion.

DIN 66134
(1998-02)  

Determination Of The Pore Size Distribution And The Specific Surface Area Of Mesoporous Solids By Means Of Nitrogen Sorption - Method Of Barrett, Joyner And Halenda (NJH).

DIN 66135-1
(2001-06)

Particle Characterization - Micropore Analysis By Gas Adsorption - Part 1: Fundamentals And Testing Procedure.

DIN 66135-2
(2001-06)

Particle Characterization - Micropore Analysis By Gas Adsorption - Part 2: Evaluation By Isotherms ComparisonDIN 66135-3 (2001-06) Particle Characterization - Micropore Analysis By Gas Adsorption - Part 3: Determination Of The Micropore Volume According To Dubini And Radushkevich.

DIN 66135-3
(2004-09)

Particle Characterization - Micropore Analysis By Gas Adsorption - Part 4: Determination Of Pore Distribution According To Horvath-kawazoe And Saito-foley.

UOP STANDARDS APPLICABLE TO THE CHARACTERIZATION OF POROUS SOLIDS USING QUANTACHROME INSTRUMENTS

UOP425-86

Surface Area, Pore Volume and Pore Diameter of Porous Substances by Nitrogen Adsorption (historical - SUPERSEDED, cannot find new version).

UOP945-96 

Platinum Dispersion on Platinum or Platinum/Tin Catalyst by Hydrogen-Oxygen Titration (historical - SUPERSEDED, cannot find new version).

UOP874-88

Pore Size Distribution of Porous Substances by Nitrogen Adsorption using a Quantachrome Analyzer (historical - SUPERSEDED, cannot find new version).

UOP851-08

Density of Powders and Solids by Helium Displacement.

UOP766-13

Piece Density by mercury Displacement.

UOP578-11

Automated Pore Volume and Pore Size Distribution of Porous Substances by Mercury Porosimetry.

UOP944-96

Surface Area of Fresh and Regenerated Catalyst.

UOP964-11

Surface Area, Pore Volume, Average Pore Diameter and Pore Diameter Distribution of Porous Materials by Nitrogen Adsorption.

 

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