To meet a growing need for temperature-specific measurement capabilities in porous materials characterization, Quantachrome Instruments and Oxford Instruments have collaborated in developing a new cryostat specially designed to provide the precise temperature control required for advanced gas sorption studies on the Autosorb-1. The new cryostat gives researchers the ability to easily perform gas sorption studies at any temperature between 77.4K and 200 K (-320°F and -100°F) using only liquid nitrogen as a cryogen, with >19hr hold time at 87K: unlimited analysis time when refilled.
Because the structure and reactivity of solid materials determines how their surfaces interact with gas molecules, monitoring the gas sorption process can provide valuable information about the characteristics of technologically useful solids. Routine evaluation of important materials properties that control their performance – such as surface area, size and shape of pores, chemically active sites, and many others – is possible by quantifying the gas–solid interactions through isothermal gas sorption measurements.
This advance in gas sorption capability allows scientists to make measurements across a wide range of temperatures, without the usual restriction of having only a limited number of specific temperatures using baths of different cryogenic liquids or melting solids. For example, high resolution micro/mesopore analysis by argon adsorption can be performed at 87 K without expense of liquid argon.
PowderTech Note #43
"Application of Customized Optistat® DN Cryostat for Advanced Adsorption and Structural Characterization Studies".To receive a copy of Tech Note #43, please send your
request with your full contact details to: qc.support@quantachrome.com
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